Factors Causing Instability of the Detection System in Infrared Carbon & Sulfur

Release Time: 2026-07-29

1. Overview

The infrared carbon & sulfur analyzer is a core analytical instrument widely used in metallurgical and machinery industries. It enables rapid quantification of carbon and sulfur contents in solid materials including steel, iron, copper, alloys, carbon compounds, ores, cement, ceramics and glass.

The detection system acts as the core heart of the carbon-sulfur analyzer. Stable baseline output of the detection system is critical for reliable test results. However, multiple factors can trigger system instability, imposing high technical requirements on operators and maintenance personnel. Analyzing these unstable factors is of great significance for equipment maintenance and ensuring smooth scientific research workflows. For years, unstable detection performance has remained a common trouble for instrument users. Long-term research and equipment maintenance have accumulated valuable practical experience, which helps boost equipment utilization, guarantee on-time completion of research and production tasks, and standardize routine maintenance of infrared carbon-sulfur analyzers.


2. Instrument Working Principle

Samples are fed into a high-frequency combustion furnace and fully oxidized under high temperature with oxygen supply, converting carbon and sulfur in the sample into CO₂, CO and SO₂.

The oxidized gas products pass through a dust removal unit and water removal purification unit, then are carried by oxygen into the sulfur detection cell for sulfur measurement. The mixed gas containing CO₂, CO, SO₂ and O₂ flows into a heated catalytic furnace, where catalytic conversion occurs: CO is transformed into CO₂ and SO₂ into SO₃. After passing through a sulfur absorption reagent tube, the gas mixture enters the carbon detection cell to measure carbon content. Residual waste gas is exhausted outdoors by the analyzer.

Output signals from carbon and sulfur detectors are processed by preamplifiers and A/D converters, then transmitted to the microcomputer system for data calculation to obtain mass percentage values of carbon and sulfur.


3. Analysis of Factors Leading to System Instability

The measured signal intensity is closely correlated with the working power supply output, infrared source radiant power, chopper motor frequency, infrared detector, A/D analog-to-digital converter, and external interference. Root causes for unstable system performance are categorized as follows:


3.1 Working Power Supply

The detection system relies on multiple power rails: ±15 V, 5.5 V, 24 V and 5 V, which are fundamental to normal instrument operation. Abnormal circuit performance and output fluctuation arise from two main issues:

  1. Aging of electronic components causes unstable output and excessive ripple voltage. Normal power supply fluctuation tolerance is ±10%; readings exceeding this range indicate abnormal status.
  2. Damaged components lead to zero output or distorted waveform signals. Faulty parts can be identified by measuring voltage at key circuit nodes and comparing with standard nominal values.

3.2 Infrared Light Source

Infrared radiation emitted by the light source is proportional to radiant power. Any variation in radiant power directly changes signal output and shifts the detector baseline — baseline readings will rise or fall synchronously with infrared intensity changes.
Three typical causes of unstable infrared radiation signals:

  1. Gradual aging of the light source reduces radiant output and lowers signal amplitude. Baseline values of carbon and sulfur detectors will drop continuously, triggering instrument alarms once readings fall below the normal range.
  2. Broken or desoldered heating filaments cut off signal output entirely. Verify the filament resistance (standard value approx. 5 Ω) for troubleshooting.
  3. Cold solder joints or oxidized power plugs create poor contact. Variable contact resistance leads to drastic random fluctuations of output signals, a frequently overlooked failure mode.

3.3 Chopper Motor

The chopper motor modulates continuous infrared light into fixed-frequency pulse signals before entering the detector. This optical modulation design ensures stable signal amplification by subsequent circuits. Malfunction of the motor results in weak or complete loss of detector signals, mainly due to:

  1. Motor stall: either power supply failure or mechanical jamming of the chopper blade assembly.
  2. Long-term mechanical wear enlarges shaft sleeve clearance, causing unstable blade rotation. Blades may collide with the detection cell wall and become stuck.
  3. Deviation of the motor’s modulation frequency from nominal values leads to uneven light transmission through the aperture, resulting in fluctuating or zero received signals at the detector.

3.4 Infrared Detector

The infrared detector is a critical core component of gas analyzers, converting infrared radiant optical signals into electrical signals. Stable ambient temperature must be maintained during operation to avoid interference noise. Common failures include:

  1. Complete component damage with zero signal output.
  2. Aging reduces sensitivity and introduces high noise floor in output signals.
  3. Oxidized solder joints and cold solder connections cause unstable signal transmission.

3.5 Preamplifier

The preamplifier amplifies weak signals from the detector, filters noise and performs DC amplification. Minor abnormalities in any part of this subsystem distort final output signals. Common faults:

  1. Degraded performance of the micro-signal amplifier; prioritize checking filter capacitors and grounding integrity during inspection.
  2. Poor contact of zero-adjustment and gain potentiometers. Rotate potentiometers back and forth several times regularly to restore good contact.
  3. Degraded amplification gain of the quad operational amplifier leads to low final analytical readings.

3.6 A/D Conversion Board

Voltage signals are sampled via a 16-bit acquisition chip, converted to digital signals by the A/D converter and sent to the computer for processing. Interference during this stage distorts real-time monitoring, integration and calculation of sample test data. Key triggers:

  1. Aging components on the A/D board degrade performance, increase interference noise and scramble digital signals.
  2. Poor instrument grounding introduces external electromagnetic interference, resulting in missing sampled data.
  3. Loose contact between the A/D board and bus slot causes loss of collected test data.

4. Conclusion

Analysis of these instability factors provides effective solutions for common faults including aged electronic components, degraded performance, zero/unstable signal output, excessive noise, missing or lost sampling data. Resolving these issues greatly improves equipment utilization efficiency and guarantees stable long-term operation of infrared carbon & sulfur analyzers.




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